384
International RILEM Conference on Materials, Systems and Structures in Civil Engineering
Conference segment on Service Life of Cement-Based Materials and Structures
22-24 August 2016, Technical University of Denmark, Lyngby, Denmark
[10] Carette J., Staquet S. Monitoring the setting process of mortars by ultrasonic P and S-
wave transmission velocity measurement, Construction and Building Materials, 2015, 94,
196-208
[11] Delsaute, B., Boulay, C., Granja, J., Carette, J., Azenha, M., Dumoulin, C., Karaiskos,
G., Deraemaeker, A., & Staquet, S. Testing Concrete E-modulus at Very Early Ages Through
Several Techniques: An Inter-laboratory Comparison, Strain, 2016, 52, 91-109
[12] C. Boulay, J.-L. Andre, J.-M. Torrenti, Draft operating protocol to determine the level of
heat released during cement hydration on a concrete specimen placed in a quasi-adiabatic
calorimeter designed for concretes (QAB), BLCPC, 278 (2010), pp. 37–42
[13] Broda, M.; Wirquin, E. & Duthoit, B. Conception of an isothermal calorimeter for
concrete: Determination of the apparent activation energy, Materials and Structures,
2002, 35, 389-394
385
International RILEM Conference on Materials, Systems and Structures in Civil Engineering
Conference segment on Service Life of Cement-Based Materials and Structures
22-24 August 2016, Technical University of Denmark, Lyngby, Denmark
CONCRETE DRYING: EFFECTS OF BOUNDARY CONDITIONS AND
SPECIMEN SHAPE
Jérôme Carette
(1,2)
, Farid Benboudjema
(1)
, Georges Nahas
(2)
, Kamilia Abahri
(1)
, Aveline
Darquennes
(1)
, Rachid Bennacer
(1)
(1) LMT-Cachan / ENS Cachan / CNRS / Université Paris Saclay, Cachan, France
(2) IRSN, Fontenay-aux-Roses, FRANCE
Abstract
In the framework of the ODOBA project, representative structures in reinforced concrete are
submitted to various types of durability distress, in order to have elements of knowledge on
pathologies which could develop in the course of time. Among studied issues are the alkali-
aggregate reaction (AAR) and the delayed ettringite formation (DEF), which appear after a
large induction period, but develop then quickly, inducing irreversible structure damage.
These issues are closely related to the water distribution and to the surrounding humidity.
Controlling the processes of drying and wetting of concrete is of major importance in this
regard. However, the mechanisms at their origin are currently not well established and
modelled. This work is a preliminary study aiming at identifying the main mechanisms in
play during drying-wetting cycles through a coupled experimental-numerical study of the
humidity gradient inside concrete. In this paper, the drying of various concrete samples is
cautiously studied through refined measurement of the mass loss and internal relative
humidity distribution. Various sample sizes and shapes are tested. A simulation strategy is
described, including the modelling of water vapour diffusion and liquid water permeation.
The introduction of a boundary layer at the drying interface improves the mass variation
prediction.
1. Introduction
In the framework of the pre-ODOBA ENSC/IRSN and ODOBA project of the IRSN (French
Institut de Radioprotection et de Sûreté Nucléaire), representative structures of reinforced
concrete will be built on the IRSN Cadarache nuclear research centre. In these structures will
be developed pathologies of concrete such as swelling reactions (internal sulphate attack
(ISA) and alkali-aggregate reaction (AAR)). The concrete used in the construction of these
structures are chosen by equivalence to the concrete used in the studied nuclear facilities.
These issues usually develop after a very long induction period (10 to 30 years).
Unfortunately, after the onset of signs of swelling, development is very rapid with
386
International RILEM Conference on Materials, Systems and Structures in Civil Engineering
Conference segment on Service Life of Cement-Based Materials and Structures
22-24 August 2016, Technical University of Denmark, Lyngby, Denmark
consequences for the safety functions of these structures. These issues are highly dependent
on the presence of water in the pore system of concrete. Therefore, control of the process of
drying-wetting becomes an important parameter, which remains the object of scarce results in
the literature. Indeed, there remain questions regarding the mechanisms involved. Thus, it is
difficult to simulate the distribution of the water content in concrete models, which leads to
difficulties in quantifying the deformation gradients due to the swelling reactions (ISA,
AAR).
This work aims at identifying the main mechanisms in play during drying-wetting cycles
through a coupled experimental-numerical study of the humidity gradient inside concrete. In
this paper, the drying of various concrete samples is cautiously studied through refined
measurement of the mass loss and internal relative humidity distribution. Various sample
sizes and shapes are tested. A simulation strategy is described, including the modelling of
water vapour diffusion and liquid water permeation [1, 2]. A limited amount of samples were
tested in this study. In addition, many parameters of the model were determined by other
authors on the same concrete. Therefore, this study must be considered as a preliminary
methodology for the monitoring and simulating the drying of concrete rather. Additional
ongoing tests will provide more information regarding further validation of the suggested
model.
2. Experimental
setup
2.1. Mix design
The tested concrete composition is referred to as B11 concrete. This concrete, which
composition and major properties are shown in Table 1, is used because it is equivalent to the
concrete actually used in French internal nuclear power plant vessels. In addition, it has been
widely studied in previous studies [1] and its properties are therefore mostly known.
Table 1: (left) B11 mix design (right) B11 concrete main properties
[t/m
3
]
B11
[kg/m³]
w/c
[-] 0.573
Cement
(CEM II Airvault Calcia)
3.1 336
[t/m
3
] 2.324
Sand (0/4)
2.572
740
Slump
[cm] 8-11
Aggregates (4/12,5)
2.57
303
Porosity
[-]
13.2-
13.8
Aggregates (10/20)
2.57
752
f
c
(28 days)
[MPa] 46.5
Water
1 193
f
t
(28 days)
[MPa] 3.29
Superplasticizer
(Plastiment
HP)
1.185 10
-
3
1.174 E (28 days)
[GPa] 31.34
2.2. Curing conditions
In order to submit all the concrete specimens to the same curing conditions (temperature T
and relative humidity RH), à large storage bin was developed. The climatic chamber was
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