Technical Specification of Niobium sheets



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TATA INSTITUTE OF FUNDAMENTAL RESEARCH

Homi Bhabha Road, Colaba, Mumbai – 400 005.

A Deemed University
Telephone : +91-22-2278 2316/2886/2887/2888 Email : psmurthy@tifr.res.in

Purchase Fax : +91-22-2280 4566 : sheela@tifr.res.in

Website : www.tifr.res.in : madhuram@tifr.res.in

: mayraj@tifr.res.in

PUBLIC TENDER NO. : TFR/PD/IM9-268/PUB

DUE DATE : 24.12.2009

TENDER FEE : Rs. 500/-

COST OF TENDER : Approx. Rs.150 lakhs

TYPE OF TENDER : TWO PART

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DESCRIPTION OF MATERIAL

High quality Nb material ASTM B393-05, RR300

Of the following sizes:

1. Nb sheet: 120 cm x 120 cm x 0.25 cm … 11 Nos.

2. Nb sheet: 60 cm x 60 cm x 0.15 cm … 4 Nos.

3. Nb rod: 7 cm dia x 100 cm long rod

As per our technical specifications

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Closing time and date : 13.00 Hours on 24.12.2009
Tender will be open at : 14.00 Hours on 24.12.2009
Both Technical Bid (Part A) and Commercial Bid (Part B) to be submitted within the due date and time in separate envelopes and marked on top as either Part A or Part B. These two sealed envelopes should be further put in one Master Envelope superscribed with the Tender No., Due Date in Bold Letters.
Please see attached sheet for conditions of tender.


P. S. MURTHY

Purchase Officer

Ref.: TFR/PD/IM9-268/PUB

Technical Specification of Niobium sheets

Table of Contents



1. Scope of the technical specification

2. Scope of the Tender

3. Eligibility criteria for the bidders

3.1 Qualified Manufacturers of the Material

3.2 Authorized Dealers of the Qualified Manufacturers of the Material

4. General conditions for tendering and contracting

4.1 Tender Procedure

4.1.1 Technical Questionnaire
4.1.2 Details of the original manufacturer and catalogue of the offered material.
4.1.3 Details of the handling agencies in India


4.1.4 Validity of offer

4.2 Purchase Order Execution

4.2.1 Purchase Order Distribution

4.2.2 Processing of Purchase Order by the Vendor

4.3 Minimum Order Quantity

4.4 Cost calculation for comparison purpose

5. Technical requirements

5.1 Material Designation and Grade

5.2 Applicable Documents

5.3 Properties and Testing

5.3.1 Chemical composition

5.3.2 Electrical requirements

5.3.3 Mechanical properties

5.3.4 Metallurgical Requirements

5.3.5 Surface Finish

5.4 Inspection and Testing

5.4.1 Chemical composition

5.4.2 Residual resitivity ratio

5.4.3 Mechanical measurements

5.4.4 Micrographs

5.4.5 Surface Finish

5.5 Tests Examination and Certification

5.5.1 Test reports

5.5.2 Inspection

6. Quantity

7. Delivery and acceptance

7.1 Delivery Terms

7.2 Delivery Schedule

7.3 Packing and Transport to TIFR

7.4 Acceptance

8. Mandatory Technical questionnaire

Table­ A.1: General Information

Table­ A.2: Technical Information

Ref.: TFR/PD/IM9-268/PUB



1. SCOPE OF THE TECHNICAL SPECIFICATION

This specification lists the technical requirements for supply of Niobium sheets as per dimensions and properties listed in this specification and conforming to ASTM B391, “Niobium and Niobium Ingot Alloys”, R04200­vType 1, reactor grade unalloyed niobium with additional requirement of RR300 and overriding requirements as specified herein.



2. SCOPE OF THE TENDER

  • This specification covers the technical requirements for supply of Niobium sheets. The scope of work includes:

  • Supply of material according to this technical specification,

  • Acceptance tests and supply of test certificates for all the tests mentioned in this document, and Safe packaging and transport to the Purchasers site.

3. ELIGIBILITY CRITERIA FOR THE BIDDERS

The only eligible bidders are as follows:



3.1 Qualified Manufacturers of the Material

The material manufacturers are eligible to bid if they operate under a quality management system ISO 9001: 2000 with material manufacturing (Niobium) in the scope of the certificate. The bidder shall attach a certificate to this effect with their bid. Preferably, they shall have their own sales office in India. The bidder must have qualified for supply of niobium for construction of multicell SC resonators in any of the renowned accelerator lab like DESY, KEK, INFN, CERN, Fermilab, TRIUMF, Cornell, ANL, TJNAL. The bidder may be asked to submit a document in support. The material being offered shall be manufactured using the same equipment, process and control. Any bidder whose material has not been successfully used for manufacturing of multicell SC resonators shall not qualify to bid for this tender. Quotations from niobium manufacturers only shall be accepted.



3.2 Authorised Dealers of the Qualified Manufacturers of the Material

A recent and valid authorization certificate from the qualified manufacturers for the supply of niobium sheets must be attached with the offer. Offers without valid authorization certificate will be rejected without any intimation to the bidder.



4. General Documentation for tendering and contracting

Please refer to the commercial bidding documents for complete information.



4.1 Tender Procedure

4.1.1 Technical Questionnaire

A mandatory technical questionnaire is attached with this Technical Specification (MANDATORY TECHNICAL QUESTIONNAIRE, Tables A­1 and A­2). The technical questionnaire has been prepared to eliminate correspondence with bidders for seeking clarifications on the inadequate/ incomplete/ missing information and / or for requesting mandatory documents required by the purchaser. The mandatory questionnaire shall be completely filled in, duly signed and stamped by the bidder on each page and submitted along with the bid. Offers received without fulfilling this condition will be considered as incomplete and will be rejected.

Ref.: TFR/PD/IM9-268/PUB

4.1.2 Details of the original manufacturer and catalogue of the offered material

Please specify the complete details of the original manufacturer of the offered material and give complete contact details (name, phone, email, web address, fax, postal address). It is mandatory to specify original manufacturer of the material.



4.1.3 Details of the handling agencies in India

Please specify the complete details of the handling agencies of the offered materials and give complete contact details (name, phone, email, web address, fax, postal address).



4.1.4 Validity of offer

Preferably, the offer shall be valid for 90 days.




4.2 Purchase Order Execution

4.2.1 Purchase Order Distribution

In case, the order is placed on the authorized dealers of the qualified material manufacturers then a copy of the purchase order will be sent to the material manufacturer as well.



4.2.2 Processing of Purchase Order by the Vendor

  • The Vendor shall give an Order Acceptance within 10 days of receipt of the Purchase Order. If the Vendor is an authorised dealer, then this Order Acceptance shall be accompanied with three documents:

  • A duly signed and stamped legible copy of authorised dealers’s purchase order on the material manufacturer. The commercial part of the document may be masked.

  • A legible copy of Order Confirmation / Acceptance issued by the material manufacturer to the authorised dealer against the receipt of the authorised dealer’s purchase order. This Order Confirmation shall clearly mention the delivery period.

  • Name and contact details of material manufacturer’s personnel handling the authorised dealer’s purchase order.

  • The Vendor shall submit the status of the supply on every month from the date of Purchase Order.

    1. Minimum Order Quantity

The quantity shown in the article 6 only indicates the minimum requirements. If the quantity happens to be less than the “Minimum Order Quantity” (MOQ) of the material, then the qualified material manufacturers and their authorized dealers are requested to quote for MOQ. Purchaser reserves the right to place order for MOQ or the quantity mentioned in the article 6 depending on availability, economy and conformance to this specification.

4.4 Cost calculation for comparison purpose

Since the order quantity may change due to conditions embedded in articles 4.3, the Cost Comparison of Tender (CST) will be made on the basis of landed cost of “one kg of weight” for each item.

Ref.: TFR/PD/IM9-268/PUB

5. TECHNICAL REQUIREMENTS

5.1 Material Designation and Grade:

Material shall be Niobium sheets cold rolled & annealed as per ASTM B 391 & ASTM B 393 with additional and overriding requirements as specified herein.



5.2 Applicable Documents

Technical supply conditions shall conform to, but not be limited to, the document’s list given below:



Table­1: Applicable Standards, Latest Edition

S. No

Parameter

Description / Specification

5.2.1

ASTM B­391

Niobium and Niobium Ingot Alloys

5.2.2

ASTM B­393

Standard Specification for Niobium and Niobium Alloy Strip, Sheet, Foil and Plate

5.2.3

ASTM B392-03

Standard specification for Niobium and Niobium alloy bar, rod and wire

5.2.4

ASTM E­112

Standard method for determining the average grain size

5.2.5

ASTM E­8

Method of tension testing of metallic materials

5.3 Properties and Testing

5.3.1 Chemical composition

Each lot of annealed Nb sheet shall conform to the following requirements for chemical composition for RRR 300 quality:



Element

Max. parts per million

(weight ppm)



Ta

≤ 500

W

≤ 70

Ti

≤ 40

Fe

≤ 30

Si

≤ 30

Mo

≤ 50

Ni

≤ 30

All other metallic impurities should be < 30 ppm each. In addition, each niobium sheet (final product) shall conform to the following requirements for dissolved interstitial elements:

Element

Max. parts per million

(weight ppm)



O

≤ 10

N

≤ 10

C

≤ 10

H

≤ 2

The method of measurement of chemical composition shall be according to Section 5.4.1

Ref.: TFR/PD/IM9-268/PUB

5.3.2 Electrical Requirements

The final product shall have a measured Residual Resistivity Ratio (RRR) value as specified in article 6. This requirement overrides the chemical composition requirement in Section 5.3.1, since the combined contributions of the impurities as listed in the above table would produce an RRR value substantially below the required value. The method of measurement of the RRR value shall be specified in Section 5.4.2.


5.3.3 Mechanical properties

The final product shall conform to the following mechanical properties at room temperature as per ASTM E­8:

The difference in yield strength and elongation in the longitudinal (rolling direction) and transverse directions shall be minimum possible and the difference shall be stated in the quotation. The purchaser reserves the right to use it as a selection criteria, in case, other properties are met in the offers. For the tensile measurement, the rate­ of­ strain shall not exceed 0.010 inch/inch minute through the 0.2% offset yield strength. The rate ­of ­strain may be increased to 0.05 inch/inch­minute thereafter. The method of measurement shall be according to Section 5.4.3.
5.3.4 Metallurgical Requirements

The final product shall be at least 95% recrystallized and shall exhibit uniform size and equiaxed grains that are predominantly ASTM #6 (0.045 mm) with no grains larger than ASTM #5 (0.064 mm) locally. The method of measurement shall be according to Section 5.4.4.



5.3.5 Surface Finish

The material shall be delivered in fully annealed condition with an “as etched” surface (free of oxide inclusions, cracks, blisters or laminations), with both surfaces having a clean “metallic” looking finish (metallic blank) and a surface roughness Rt<15 µm. The delivered material shall be free of injurious internal or external imperfections of a nature that would interfere in the deep drawing operation of RF cavity components. Particular care should be taken in the final rolling and subsequent handling to avoid the inclusion and embedding of particles of foreign material in the surface of the sheets. The method of measurement shall be according to Section 5.4.5.



5.4 Inspection and Testing

The tests listed below are the minimum required and are not intended to supplant any controls, examinations, inspections, or tests normally employed by the seller to assure the quality of the product. A minimum of two samples per sheet shall be taken from two sheets per each lot of Nb sheet covered by this specification.



5.4.1 Chemical composition

The method of measurement of chemical composition shall be by x­-ray emission spectroscopy (ASTM E­902), spark source mass spectrometry (ASTM E­304) or other instruments with demonstrated equal sensitivity and accuracy, including dc plasma spectroscopy, optical emission spectroscopy or inductively coupled plasma spectroscopy.



5.4.2 Residual Resistivity Ratio

RRR is defined as the ratio of D.C. bulk electrical resistivity at 293K and at 4.2K when the material is in a normal, non­-superconducting state. Samples for RRR measurement shall be approximately 2.0 mm x 5.0 mm x 50.0 mm in size. The high temperature measurement shall be made at 293 ± 1 K. The low temperature measurement may be made by one of two methods. It may be made above the critical temperature (9.2K) at say 10 K, in which case the measurement temperature must be recorded. Alternatively, the low temperature resistance measurement may be made at 4.2K, in which case the measurement must be made while the sample is in a magnetic field greater than 10,000G in order to assure that it is fully in the normal­ conducting state and not in a superconducting state.



5.4.3 Mechanical Measurements

Measurements shall be performed in accordance with ASTM E­8 to determine Yield strength, Tensile strength and Elongation. Both longitudinal (to the rolling direction) and transverse (perpendicular to rolling direction) sections shall be examined as described in the following paragraph. For the tensile measurements, the rate of strain shall not exceed 1%/minute through the 0.2% offset yield strength. The rate of strain may be increased 5%/minute thereafter. Hardness (HV) has to be measured after final annealing for each sheet. The grain size shall be measured in accordance with ASTM E­112, Section 3.1.3.



5.4.4 Micrographs

Photomicrographs shall be obtained as per ASTM Method E 883 as follows: Both through­thickness longitudinal (along rolling direction) and transverse (perpendicular to rolling direction) sections shall be prepared as per ASTM E3. One representative photomicrograph at X500 magnification per sample orientation (longitudinal and transverse) and one representative photomicrograph at X50 magnification per sample orientation shall be taken.



5.4.5 Surface Finish Inspection

For the surface finish, both sides of each sheet must pass a 1X visual inspection as follows: Inspections must be performed with the naked eye or correction to 20­20 vision, at a distance of no more than 10 inches and with the aid of a 100 Watt light source. Magnifying aids may be used to determine the following causes, any of which are cause for whole or part rejection:

•Pores, indentations or "orange peeling".

•Scratches deeper than .001 inch.

•Dirt or grease deposits.
5.5 Tests Examination and Certification

The seller shall maintain a documented quality assurance program that will insure that each item offered for acceptance or approval conforms to the requirements herein. A Quality Assurance plan must be submitted with the proposal and must be approved prior to the award of the contract.



5.5.1 Test Reports

Each of the following tests shall be done. The reports of the tests shall be sent to the purchaser at the time of material shipment.



5.5.1.1 Chemical analysis ( ingot and final product); specific values per section 5.3.1.

5.5.1.2 Residual resistivity ratio; specific values per Section 5.3.2.

5.5.1.3 Mechanical properties, specific values per Section 5.3.3

5.5.1.4 Grain size; specific values per Section 5.3.4.

5.5.1.5 Surface Finish per Section 5.3.5

5.5.1.6 Micrographs per Section 5.4.3
5.5.2 Inspection

TIFR reserves the right to have its technical or procurement representatives witness manufacturing steps, tests and inspections established under the seller's quality assurance program to demonstrate compliance with the specifications. Any information of a proprietary nature must be identified in the bid process.

Ref.: TFR/PD/IM9-268/PUB

6. QUANTITY

The dimensions and quantity of niobium sheets are mentioned in below. The sheet flatness shall be according to ASTM B708­, 2% or better.



Table­ 2: Quantity

Sr

Material

Unit

Qty

1

Nb sheet: 120 cm ± 0.5cm × 120 cm ± 0.5 cm × 0.25 cm ± 0.01cm

No.

11

2

Nb sheet: 60 cm ± 0.5 cm × 60 cm ± 0.5 cm × 0.15 cm ± 0.01cm

No.

4

3

Nb rod : 7 cm dia ± 0.1cm × 100 cm ± 0.5 cm

No.

1

7. Delivery and Acceptance

7.1 Delivery Terms

7.1.1 The Domestic Offers

The offer shall only be made on F.O.S. (free on stores)TIFR, only.

The excise and VAT shall be mentioned separately in a cost break up. Please note that excise duty exemption certificate cannot be issued for purchase of raw materials.

7.1.2 Overseas Offers

Preferably, the offer shall be made on the F.O.B. basis.



7.2 Delivery Schedule

The items shall be delivered to TIFR premises within 6 months of placement of purchase order. Offers quoting more that 6 months’ delivery period would be considered after adding 2% of the offered cost for each completed month for performing cost comparison of the offers. Offers quoting more than 10 months of delivery period may not be considered.



7.3 Packing and Transport to TIFR

7.3.1 The material shall be coated on all sides by an adhesive PVC coating. Note that the PVC coating material should not contain any silicone. The material shall be individually wrapped or paper interleaved with non­abrasive, anti­-tarnish paper to prevent surface damage. Wrapped sheets shall be packed for shipment in a way to prevent damage during normal hazards to shipment.

7.3.2 The material shall be delivered as packed at TIFR, Mumbai India.

7.4 Acceptance

Supplier will sample two sheets from each lot. Two samples will be cut from each sheet. Supplier will test one sample for the required attributes and the other sample will be provided to TIFR for obtaining approval prior to the supply of the material. TIFR will accept the material on the basis of test certificates and samples test results.

All documentation as per 5.5.1 should be submitted to TIFR. Pre-­dispatch inspection will be carried out. An identification system shall be carried with material to provide cross­reference to the test documentation.

Ref.: TFR/PD/IM9-268/PUB



8. MANDATORY TECHNICAL QUESTIONNAIRE

(TO BE FILLED IN BY THE BIDDER & SUBMITTED ALONGWITH THE OFFER)



Instruction­-1

Table A.1 and Table A.2: The rightmost column should be filled in by the Bidder.

Instruction­-2

Failure to submit a fully completed, duly signed and stamped questionnaire will result in the rejection of the offer.

Instruction­-3

Wherever,the response isYes/No, please strike out the inapplicable response.

Table­ A.1: General Information

Qualification of the Material Manufacturer

A.1.1.

Name of the Material Manufacturer




A.1.2.

Contact details of the manufacturer (Give full address, email, phone and fax numbers.)




A.1.3.

Do the manufacturers have their own corporate office in India? (Give full address, email, phone and fax numbers.)

Yes/No

A.1.4.

Do you have ISO 9001:2000 certification as mentioned in article 3.1?

Yes/No

Qualification of Authorized Dealers of the Qualified Manufacturers


Delivery, Service and Warranty

A.1.7.

Delivery Period

……….months after confirmed order.

A.1.8.

Delivery Terms

F.O.S, TIFR OR CIF,…………....(Destination Port)

A.1.9.

Do you certify that you will be able to supply the material within the delivery period mentioned in your offer?

Yes/No

A.1.10.

If you are an authorised dealer, then have you confirmed the availability of the offered material within the offered delivery period with the material manufacturer?

Yes/No

Ref.: TFR/PD/IM9-268/PUB

Table­A.2: Technical Information


S.No.

Question

Response

A.2.1.

Whether you will provide mill certificate or test certificate issued by an approved lab?

Mill certificate / test certificates by approved lab (strike out the inapplicable response)

A.2.2.

Do you have testing facility required for testing material as specified in the specifications? If not where do you propose to do these tests?

Yes/No If no then provide name, address and contact details of the material testing lab.

A.2.3.

Is the purity of niobium per article­ 6?

Yes/No

A.2.4.

Will you provide certificates for Chemical composition, Mechanical properties, Metallographic examination, Ultrasonic Examination and Intergranular corrosion test?

Yes/No

Signature:

Name of Authorised Signatory:


Stamp of the bidding firm:


TATA INSTITUTE OF FUNDAMENTAL RESEARCH

(Deemed University)

National Centre of the Government of India for Nuclear Science and Mathematics

HOMI BHABHA ROAD, COLABA, MUMBAI – 400 004



(PURCHASE SECTION)
Terms and Conditions

  1. PART “A” (Technical Bid) consisting of Technical Bid & Commercial Terms and PART “B” (Commercial Bid) consisting of only Price shall be submitted in separate sealed envlopes duly superscribed with the tender enquiry number, and the due date in bold letters, addressed to the Purchase Officer, Tata Institute of Fundamental Research, Homi Bhabha Road, Colaba, Mumbai – 400 005. The envelopes should be clearly marked on top as either PART “A” or PART “B”. The two sealed covers should be further put in a master cover superscribed with the Tender Enquiry No., Due Date in bold letters, addressed to the Purchase Officer, Tata Institute of Fundamental Research, Homi Bhabha Road, Colaba, Mumbai – 400 005. The sealed master envelop has to be delivered by hand/courier at the security Gate Officer of TIFR on or before 13.000 hrs on the due date specified. The technical bid will be opened in the presence of attending tenderers at 14.00 hrs on the due date in the Purchase Section.




  1. In case the PART ‘A’ and Part ‘B’ bids are not sealed in separate envelopes the tender will be rejected.




  1. The technical bid should not contain any indication of the price.




  1. After scrutiny of Technical Bids, Commercial bids of only those who are shortlisted on technical basis will be opened at on later date. The opening date, time and venue will be intimated to the technically successful bidder.




  1. Tender Forms can be obtained from the Purchase Section on payment of the tender fees (non-refundable) of Rs.500/- by cash/Demand Draft in favour of Tata Institute of Fundamental Research, Mumbai, to the cashier, Accounts Department on any working day between 11.00 a.m. to 12.30 p.m. and 1.00 p.m. to 3.00 p.m.




  1. The firm who wishes to download the specifications, terms and conditions may do so. While submitting the quotation, a DD of Rs.500/- for each tender drawn in favour of Tata Institute of Fundamental Research, Mumbai may please be enclosed along with Technical Bid. Foreign Suppliers prepare advance cheque for US$100/-.




  1. Quotations must be valid for a period of 180 days from the date of your quotation.




  1. Tenders containing correction, overwriting will not be considered.




  1. Tenderer should sign on all the pages of the technical bid and the price bid.




  1. Offer should be on the basis of Ex-works, duly packed airworthy.




  1. If equipment offered is to be imported, arrangements for import will be made by us.



  1. Tenders who do not comply with any of the above conditions are liable to be rejected.




  1. The Institute shall be under no obligation to accept the lowest or any other tender received in response to this tender notice and shall be entitled to reject any tender without assigning any reason whatsoever.




  1. We reserve the right to place the order for part/reduced quantity than what is specified in the tender.




  1. Our standard Payment terms are as follows:

- Up to maximum of 90% against shipment of the equipment/materials (through Letter of Credit)

- Balance 10% of the order value will be released on receipt, installation, commissioning and acceptance of the equipment/machinery.



In case any supplier wants advance payment for mobilization the same can be released on submission of bank guarantee for the equal amount valid till the date of shipment of the equipment/material.
16. As per CVC guidelines No Agency commission will be paid by TIFR
PURCHASE OFFICER
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